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Merck
CN

13081-U

Supelco

玻璃填充 GC 色谱柱(适用于Agilent,配置“A”)

phase 10% FFAP + 1% H3PO4, matrix 100/120 Chromosorb W AW support, L × O.D. × I.D. 6.0 ft (1.8 m) × 1/4 in. × 2.0 mm

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物料

glass column

制造商/商品名称

Agilent

参数

60-225 °C temperature (isothermal or programmed)

技术

gas chromatography (GC): suitable

长度 × 外径 × 内径

6.0 ft (1.8 m) × 1/4 in. × 2.0 mm

基质

100/120 Chromosorb W AW support

基质活性基团

10% FFAP + 1% H3PO4 phase

色谱柱类型

packed GC

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一般描述

In a packed column, the carrier gas percolates through the porous bed and separation is achieved by moving the solutes apart. Packed columns are made up of two main materials; stainless steel and Pyrex glass. Pyrex glass columns are shaped as desired by coiling at about 700°C. Glass column are in some cases treated with silanizing reagent to eliminate the surface hydroxyl groups which becomes catalytically active and produce asymmetric peaks. Chromosorb W, a fragile white solid prepared by heating the diatomaceous earth with a flux. The resulting fine structure is cemented over glass which results in large and irregular pores. Chromosorb W provides a relatively inert surface and is suitable for polar compounds. Chromosorb W needs to be acid washed (AW) followed by silanized to make it less active and more inert.
Use a glass column for applications where high inertness is required, such as for the analysis of active analytes. All glass columns undergo a proprietary high temperature silanization to ensure inertness. This column fits Agilent 5880, 5890, 6890. 7820, and 7890 (configuration A, on-column injection, all detectors except TCD).

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分析证书(COA)

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Satinder Ahuja
Chromatography and Separation Science, 137-138 (2003)
Ian A. Fowlis
Gas Chromatography, 27-27 (2008)
Raymond P. W. Scott
Introduction to Analytical Gas Chromatography (1997)

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