物料
glass column
技术
gas chromatography (GC): suitable
长度 × 外径 × 内径
6.0 ft (1.8 m) × 1/4 in. × 2.0 mm
基质
80/100 Chromosorb W HP support
基质活性基团
3% OV-1 phase
色谱柱类型
packed GC
相容性
for use with Agilent Configuration A
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一般描述
In a packed column, the carrier gas percolates through the porous bed and separation is achieved by moving the solutes apart. Packed columns are made up of two main materials; stainless steel and Pyrex glass. Pyrex glass columns are shaped as desired by coiling at about 700°C. Glass column are in some cases treated with silanizing reagent to eliminate the surface hydroxyl groups which becomes catalytically active and produce asymmetric peaks. Chromosorb W is a fragile white solid prepared by heating the diatomaceous earth with a flux. The resulting fine structure is then cemented over glass which results in large and irregular pores. HP is the classification of a support as high performance grade.
Use a glass column for applications where high inertness is required, such as for the analysis of active analytes. All glass columns undergo a proprietary high temperature silanization to ensure inertness. This column fits Agilent 5880, 5890, 6890. 7820, and 7890 (configuration A, on-column injection, all detectors except TCD).
应用
Chromosorb W HP support packed glass GC colum was used in separating the Me3Si derivatives of the phenolic acids.
法规信息
新产品
此项目有
Robert L. Grob and Eugene F. Barry
Modern Practice of Gas Chromatography, 76-76 (2004)
Free, esterified, and insoluble-bound phenolic acids. 1. Extraction and purification procedure.
Krygier
Journal of Agricultural and Food Chemistry, 30, 330-334 (1982)
Ian A. Fowlis
Gas Chromatography, 27-27 (2008)
Raymond P. W. Scott
Introduction to Analytical Gas Chromatography (1997)
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