form
solid
packaging
bottle of 50 g
parameter
0-180 °C temp. range
technique(s)
gas chromatography (GC): suitable
matrix active group
Bentone 34 phase
solubility
toluene: soluble
column type
packed GC
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General description
合成的产品更纯净,分子量范围窄,不含用作 GC 固定相的痕量催化剂或杂质。
GC methods are divided into two classes depending on the nature of stationary phases; gas-solid chromatography (GSC) and gas-liquid chromatography (GLC). GSC has solid adsorptive material and solute particles are removed from mobile phase by electrostatic forces. GLC has a thin layer of liquid coated or bonded on the surface of an inert particle or on the walls of the column where solute particles are retained in the liquid phase based on their partition coefficients. The primary necessity of a stationary phase is to provide sample separation sustaining phase integrity over a reasonable period of time. It should be stable for the chemical and thermal changes. Selectivity, peak symmetry, analysis time, degree of separation, peak tailing are few parameters that should be considered before choosing a stationary phase. Bentone 34 is a bentonite treated with dimethyloctadecylammonium salts which has broad applications in GC. It can differentiate between isomers of many aromatic compounds and cycloalkane derivatives. It can also be modified with silicone oil in order to improve the peak symmetry.
Application
Bentone 34 may be used as column coating, using a benzene-methanol (9:1) mixture as dispersion agent to analyse cresol mixtures.
仅试剂盒组分
产品编号
说明
- Bentone® 34
存储类别
13 - Non Combustible Solids
wgk
WGK 2
flash_point_f
Not applicable
flash_point_c
Not applicable
ppe
Eyeshields, Gloves, type N95 (US)
H. Rotzsche
Stationary Phases in Gas Chromatography (1991)
Analysis of isomeric cresols by gas chromatography.
Nardillo, A. M.,
Chromatographia, 32, 457-460 (1991)
David B. Troy, Paul Beringer
Remington: The Science and Practice of Pharmacy, 605-605 (2006)
James P. Lodge, Jr.
Methods of Air Sampling and Analysis, 98-98 (1988)
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