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Merck
CN

24010

SP-2250

L × I.D. 30 m × 0.25 mm, df 0.20 μm

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eCl@ss:
32119290
UNSPSC Code:
41115710
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material

fused silica

agency

meets requirements for USP G3

parameter

0-250 °C temperature (isothermal or programmed)

Beta value

313

df

0.20 μm

technique(s)

gas chromatography (GC): suitable

L × I.D.

30 m × 0.25 mm

matrix active group

Non-bonded; poly(50% phenyl/50% methyl siloxane) phase

column type

capillary intermediate polar

General description

Application: The SP-2250 column is a non-bonded 50% phenyl polymer. It is highly effective for the analysis of polar compounds.
USP Code: This column meets USP G3 requirements.
Phase:
  • Non-bonded
  • Poly(50% phenyl/50% methyl siloxane)
Temp. Limits:
  • 0 °C to 250 °C (isothermal or programmed)

Application

Capillary column coated with SP®-2250 (methyl silicone-phenyl silicone, 1:1) stationary phase may be used in gas chromatographic analysis of azaarenes (benzacridines and dibenzacridines).

Other Notes

We offer a variety of chromatography accessories including analytical syringes

Legal Information

SP is a registered trademark of Sigma-Aldrich Co. LLC

法规信息

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W Löscher
Therapeutic drug monitoring, 4(3), 315-318 (1982-01-01)
A rapid method was developed for the determination of diazepam, desmethyldiazepam, oxazepam, and 3-hydroxydiazepam (temazepam) in human plasma using electron capture gas chromatography. Following a single extraction with benzene from 0.2 ml plasma, diazepam and its metabolites were quantitated on
O W Lau et al.
Methods and findings in experimental and clinical pharmacology, 13(7), 475-481 (1991-09-01)
A gas-liquid chromatographic method was developed for the simultaneous assay of six local anesthetics, including amethocaine, bupivacaine, etidocaine, lignocaine, mepivacaine and prilocaine, in biological samples. These drugs and internal standard (clomipramine) in basified samples were extracted into 5 ml n-hexane
D Courtot
British journal of sports medicine, 10(3), 143-146 (1976-10-01)
At the request of the Service des Haras, our laboratory works on the toxicological problems of the sport-horse. These studies have resulted in the setting up of an anti-doping control for equestrian competitions of various types, not only flat racing.
D F Tomkins
Journal - Association of Official Analytical Chemists, 70(6), 1056-1058 (1987-11-01)
An isothermal gas chromatographic method for measuring alachlor in Micro-Tech (microencapsulated) formulations was tested by 5 collaborators. The samples were prepared in acetone, and alachlor was determined using a gas chromatographic column of 10% SP-2250 on 100-120 mesh Supelcoport. Di-n-pentylphthalate
J E Wallace et al.
Clinical chemistry, 25(7), 1296-1300 (1979-07-01)
We describe the use of electron-capture gas chromatography or reversed-phase "high-performance" liquid chromatography for concurrent analysis for diazepam and nordiazepam in serum. In the gas-chromatographic analysis our use of a new chemically deactivated stationary liquid phase, SP 2250-DB (Supelco, Inc.)

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