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Merck
CN

33037-U

BSA 衍生化级别

别名:

N,O-Bis(trimethylsilyl)acetamide

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EC Number:
233-892-7
UNSPSC Code:
12352200
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grade

derivatization grade ((GC derivatization)), derivatization grade

description

Silylation reagent

reaction suitability

reagent type: derivatization reagent
reaction type: Silylations

packaging

pkg of 1 × 25 mL

General description

BSA (N,O-Bis(trimethylsilyl)acetamide) is a powerful reagent for silyation of alkyl hydroperoxides. It reacts quantitatively under mild conditions with alcohols, amines, phenols and carboxylic acids which gives trimethylsilyl ethers and esters.

Application

BSA was used in silyation procedure of amino acid phenylthiohydantoin standards during GC analysis.

Other Notes

Reagent for 1,3-dipheylimidazolidine-2-carboxylic acid, o-ethyloxime, quinoxalone, trimethylsilyl and trimethylsilyl oximes.

signalword

Danger

Hazard Classifications

Acute Tox. 4 Oral - Flam. Liq. 3 - Skin Corr. 1B

supp_hazards

存储类别

3 - Flammable liquids

wgk

WGK 3

flash_point_f

111.2 °F - closed cup

flash_point_c

44 °C - closed cup

ppe

Eyeshields, Faceshields, Gloves, type P3 (EN 143) respirator cartridges

法规信息

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历史批次信息供参考:

分析证书(COA)

Lot/Batch Number

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D.R. Knapp
Handbook of Analytical Derivatization Reactions, 202-232 (1979)
Derivatives for the identification and quantitative determination of some keto and aldo-caroxylic acids by gas-liquid chromatography.
R A Chalmers et al.
The Analyst, 97(161), 951-957 (1972-12-01)
N.E.Hoffman and T. Killinger
Analytical Chemistry, 41, 162-162 (1969)
Mass spectrometric studies of thyroxine and related compounds. Trimethylsilyl derivatives.
A M Lawson et al.
Biomedical mass spectrometry, 1(6), 374-380 (1974-12-01)
Gas chromatographic behavior of trimethylsilylated phenylthiohydantoin amino acids.
R E Harman et al.
Analytical biochemistry, 25(1), 452-458 (1968-10-24)

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