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Merck
CN

53798-U

Supelco

Ascentis® Express Phenyl-Hexyl,2.7μm HPLC色谱柱

L × I.D. 2 cm × 2.1 mm, pk of 1 ea

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UNSPSC代码:
41115700
eCl@ss:
32110501
NACRES:
SB.52
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物料

stainless steel column

质量水平

Agency

suitable for USP L11

产品线

Ascentis®

特点

endcapped

包装

pk of 1 ea

制造商/商品名称

Ascentis®

参数

60 °C temp. range
600 bar max. pressure (9000 psi)

技术

HPLC: suitable
LC/MS: suitable
UHPLC-MS: suitable
UHPLC: suitable

长度 × 内径

2 cm × 2.1 mm

表面积

135 m2/g

杂质

<5 ppm metals

基质

Fused-Core particle platform
superficially porous particle

基质活性基团

phenylhexyl phase

粒径

2.7 μm

孔径

90 Å

pH值范围

2-9

应用

food and beverages

分离技术

reversed phase

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一般描述

由于溶质与键合相的芳香环及其离域电子发生相互作用,使Phenyl-Hexyl固定相具有独特的选择性。这种独特的芳香基选择性使其与C18和RP-酰胺固定相互补(正交)。Phenyl-Hexyl固定相也倾向于具有良好的形状选择性,这可能来自于溶质与平面环系统的多点相互作用。对于具有芳族吸电子基团(氟、硝基等)或具有离域杂环系统(如苯二氮类化合物)的溶质,通常具有更强的保留性和选择性。

法律信息

Ascentis is a registered trademark of Merck KGaA, Darmstadt, Germany

储存分类代码

11 - Combustible Solids

WGK

WGK 3

闪点(°F)

Not applicable

闪点(°C)

Not applicable

法规信息

新产品
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历史批次信息供参考:

分析证书(COA)

Lot/Batch Number

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C M Chavez-Eng et al.
Journal of chromatography. B, Analytical technologies in the biomedical and life sciences, 1011, 204-214 (2016-01-17)
An ultra-high performance liquid chromatography/tandem mass spectrometry (UPLC-MS/MS) method for the simultaneous determination of (4S,5R)-5-[3,5-bis (trifluoromethyl)phenyl]-3-{[4'-fluoro-5'-isopropyl-2'-methoxy-4-(trifluoromethyl)biphenyl-2-yl] methyl}-4-methyl-1,3-oxazolidin-2-one (anacetrapib, I) and [(13)C5(15)N]-anacetrapib, II in human plasma has been developed to support a clinical study to determine the absolute bioavailability of I.
E Lesellier
Journal of chromatography. A, 1266, 34-42 (2012-11-03)
The recent introduction of new stationary phases for liquid chromatography based on superficially porous particles, called core-shell or fused-core, dramatically improved the separation performances through very high efficiency, due mainly to reduced eddy diffusion. However, few studies have evaluated the
Ivona Lhotská et al.
Analytical and bioanalytical chemistry, 408(12), 3319-3329 (2016-03-20)
A new fast and sensitive method based on on-line solid-phase extraction on a fused-core precolumn coupled to liquid chromatography with fluorescence detection has been developed for ochratoxin A (OTA) and citrinin (CIT) determination in lager beer samples. Direct injection of
Alex D Batista et al.
Talanta, 133, 142-149 (2014-12-02)
On-line sample pretreatment (clean-up and analyte preconcentration) is for the first time coupled to sequential injection chromatography. The approach combines anion-exchange solid-phase extraction and the highly effective pentafluorophenylpropyl (F5) fused-core particle column for separation of eight sulfonamide antibiotics with similar
Dalibor Šatínský et al.
Talanta, 142, 124-130 (2015-05-25)
A new on-line SPE-HPLC method using fused-core columns for on-line solid phase extraction and large volume sample injection for increasing the sensitivity of detection was developed for the determination of insecticides fenoxycarb and cis-, trans-permethrin in surface waters. The separation

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