Synthesis of stable isotope labeled 3-acetyldeoxynivalenol.

Synthesis of stable isotope labeled 3-acetyldeoxynivalenol.

Molecular nutrition & food research (2005-10-18)

Michael Bretz, Marita Beyer, Benedikt Cramer, Hans-Ulrich Humpf

摘要

Stable isotope labeled 3-acetyldeoxynivalenol (3-AcDON) was synthesized in excellent yield from deoxynivalenol as starting material. This is the first synthesis of a stable isotope labeled type-B trichothecene suitable as internal standard for HPLC-MS/MS or GC-MS analysis of trichothecene mycotoxins. The isotopic purity of the 3-d(3)-AcDON was determined to be 94.9%.

材料

产品编号

品牌

产品描述

A6166

Sigma-Aldrich

3-乙酰脱氧雪腐镰刀菌烯醇来源于粉红镰刀菌, from Fusarium roseum

34132

Supelco

3-乙酰脱氧雪腐镰刀菌烯醇溶液, ~100 μg/mL in acetonitrile, analytical standard