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  • Convenient and efficient microwave-assisted synthesis of a methyl derivative of the fused indoloquinoline alkaloid cryptosanguinolentine.

Convenient and efficient microwave-assisted synthesis of a methyl derivative of the fused indoloquinoline alkaloid cryptosanguinolentine.

Molecules (Basel, Switzerland) (2010-07-27)
Robert M Gengan, Pitchai Pandian, Chandraprakash Kumarsamy, Palathurai S Mohan
摘要

An efficient synthesis of a methyl derivative of the indoloquinoline alkaloid cryptosanguinolentine based on microwave-assisted reactions is described. The microwave-assisted synthesis of an intermediate 4-hydroxy-2-methylquinoline yielded 86% of the desired product and other intermediates prepared yielded high % of products in shorter reaction times, under optimum conditions, as compared to traditional methods.

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Sigma-Aldrich
2-甲基喹啉, ≥95.0% (GC)
Supelco
2-甲基喹啉, analytical standard, ≥90% (GC)