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Merck
CN
  • Use of gas chromatography-mass spectrometry/solid phase microextraction for the identification of MVOCs from moldy building materials.

Use of gas chromatography-mass spectrometry/solid phase microextraction for the identification of MVOCs from moldy building materials.

Journal of microbiological methods (2003-01-18)
Loay Wady, Annicka Bunte, Christina Pehrson, Lennart Larsson
摘要

Gas chromatography-mass spectrometry/solid phase microextraction (GC-MS/SPME) was applied to identify microbial volatile organic compounds (MVOCs) in water-damaged, mold-infested building materials (gypsum board papers (n=2), mineral wool, and masonite) and in cultivated molds (Aspergillus penicillioides, Stachybotrys chartarum, and Chaetomium globosum). Three SPME fibers (65-microm PDMS-DVB, 75-microm Carboxen-PDMS, and 70-microm Carbowax-stableflex) designed for automated injection were used of which the latter showed best performance. A number of previously reported MVOCs were detected both in the building materials and the cultivated molds. In addition, methyl benzoate was identified both in the S. chartarum and A. penicillioides cultures and in the building materials. SPME combined with GC-MS may be a useful method for the determination of MVOCs emitted from mold-infested building materials.

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Supelco
SPME萃取头组件, 50/30µm DVB/CAR/PDMS, StableFlex (1 cm), needle size 23 ga, Autosampler, pk of 3, plain gray hub
Supelco
SPME萃取头组件, 50/30µm DVB/CAR/PDMS, StableFlex (2cm), needle size 24 ga, Autosampler, pk of 3, notched gray hub
Supelco
SPME萃取头组件, 50/30µm DVB/CAR/PDMS, StableFlex (1cm), needle size 24 ga, Manual Holder, pk of 3, plain gray hub
Supelco
SPME萃取头组件, 50/30µm DVB/CAR/PDMS, StableFlex (2cm), needle size 23 ga, Autosampler, pk of 3, notched gray hub
Supelco
SPME萃取头组件, 50/30µm DVB/CAR/PDMS, StableFlex (1 cm), needle size 24 ga, Autosampler, pk of 3, plain gray hub
Supelco
ORBO Carboxen-564 管, W,F,F separators, O.D. × L 6 mm × 75 mm, pkg of 25 ea, for analyte group MEK (methylethyl ketone)
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ORBO-78 400/200mg,每包 25 支, W,W,W separators, O.D. × L 6 mm × 110 mm, pkg of 25 ea
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Carboxen®1010 多孔层壁涂开管柱, L × I.D. 30 m × 0.53 mm, average thickness 30 μm
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Carbopack®吸附剂, matrix Carboxen® 1000, 60-80 mesh, bottle of 10 g
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SPME固相微萃取萃取头 Carboxen/聚二甲基硅氧烷 (CAR/PDMS), 75 μm CAR/PDMS, Fused Silica (1 cm), needle size 24 ga, Manual Holder, pk of 3, black hub
Supelco
Carboxen® 1006 多孔层壁涂开管柱, L × I.D. 30 m × 0.53 mm, average thickness 30 μm
Supelco
SPME固相微萃取萃取头 Carboxen/聚二甲基硅氧烷 (CAR/PDMS), 75 μm CAR/PDMS, Fused Silica (1 cm), needle size 24 ga, Autosampler, pk of 3, black hub
Supelco
SPME固相微萃取萃取头 Carboxen/聚二甲基硅氧烷 (CAR/PDMS), 85 μm CAR/PDMS, StableFlex (1 cm), needle size 23 ga, Autosampler, pk of 3, light blue hub
Supelco
Carboxen®1010 多孔层壁涂开管柱, L × I.D. 30 m × 0.32 mm, average thickness 15 μm
Supelco
SPME固相微萃取萃取头 Carboxen/聚二甲基硅氧烷 (CAR/PDMS), 85 μm CAR/PDMS, StableFlex (1 cm), needle size 24 ga, Manual Holder, pk of 3, light blue hub
Supelco
SPME固相微萃取萃取头 Carboxen/聚二甲基硅氧烷 (CAR/PDMS), 85 μm CAR/PDMS, StableFlex (1 cm), needle size 24 ga, Autosampler, pk of 3, light blue hub
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ORBO-93吸附管, ORBO tube I.D. × L 6 mm × 95 mm, Bed A 180 mg, Bed B 90 mg, 60/80 mesh, pkg of 25 ea
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SPME固相微萃取萃取头 Carboxen/聚二甲基硅氧烷 (CAR/PDMS), 75 μm CAR/PDMS, Fused Silica (1 cm), needle size 23 ga, Autosampler, pk of 3, black hub
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Carboxen® 1006 多孔层壁涂开管柱, L × I.D. 30 m × 0.32 mm, average thickness 15 μm
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Tenax® TA/Carboxen® 1018, glass TD tube, preconditioned, O.D. × L 1/4 in. × 3 1/2 in., Sealed with (Swagelok® End-Fittings), pkg of 10 ea
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SPME固相微萃取萃取头 Carboxen/聚二甲基硅氧烷 (CAR/PDMS), 75 μm CAR/PDMS, Fused Silica (1 cm), needle size 23 ga, Manual Holder, pk of 3, black hub
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Carbopack®吸附剂, matrix Carboxen® 1003, 40-60 mesh, bottle of 10 g
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SPME萃取头组件, 50/30µm DVB/CAR/PDMS, Metal Alloy (2cm), needle size 23 ga, Autosampler, pk of 1, plain gray hub
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Carboxen® 572 for Tobacco Smoke, Adsorbent Bed Wt: 300 mg, cartridge size 3 mL, pkg of 50 ea
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SPME萃取头组件, 50/30µm DVB/CAR/PDMS, Metal Alloy (1cm), needle size 23 ga, Autosampler, pk of, plain gray hub
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Carbopack®吸附剂, matrix Carboxen® 569, 20-45 mesh, bottle of 10 g
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2-己酮, analytical standard
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2-庚酮, analytical standard
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Carboxen® 1000 双向固相萃取管, 200 mg/mL, pk 30
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Carbopack®吸附剂, matrix Carboxen® 572, 20-45 mesh, bottle of 10 g