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Merck
CN

157260

1-羟基苯并三唑 水合物

98% dry basis wetted with not less than 14 wt. % water, for peptide synthesis

别名:

HOBt 一水合物

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关于此项目

经验公式（希尔记法）:
C6H5N3O · xH2O
化学文摘社编号:
123333-53-9
分子量:
135.12 (anhydrous basis)
MDL number:
MFCD00065690
UNSPSC Code:
12352000
PubChem Substance ID:
24849666
NACRES:
NA.22
EC Number:
219-989-7
Beilstein/REAXYS Number:
4515

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产品名称

1-羟基苯并三唑 水合物, wetted with not less than 14 wt. % water, 98% dry basis

SMILES string

[H]O[H].On1nnc2ccccc12

InChI

1S/C6H5N3O.H2O/c10-9-6-4-2-1-3-5(6)7-8-9;/h1-4,10H;1H2

InChI key

PJUPKRYGDFTMTM-UHFFFAOYSA-N

assay

98% dry basis

form

solid

quality

synthesis grade

reaction suitability

reaction type: Addition Reactions

mp

155-158 °C (lit.)

application(s)

peptide synthesis

Quality Level

200

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相关类别

Application

1-羟基苯并三唑水合物可用作以下反应的试剂：
  • 通过微波辅助的氨基酸偶联反应合成β-肽。
  • 糖肽的点合成。
它也可用作去除Fmoc（9-芴甲氧基羰基）保护基团的脱保护剂。

General description

1-羟基苯并三唑水合物是一种苯并三唑衍生物，主要用作肽合成中的偶联剂。

pictograms

FlameExclamation mark
GHS02,GHS07

signalword

Danger

Hazard Classifications

Aquatic Chronic 3 - Desen. Expl. 2 - Eye Irrit. 2

supp_hazards

EUH044

存储类别

4.1A - Other explosive hazardous materials

wgk

WGK 1

flash_point_f

314.6 °F

flash_point_c

157 °C

法规信息

监管及禁止进口产品
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历史批次信息供参考:

分析证书(COA)

Lot/Batch Number
BCCN6633
SDBB4471
SDBB1081
SDBB1080
STBL4114

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  1. Which document(s) contains shelf-life or expiration date information for a given product?

    If available for a given product, the recommended re-test date or the expiration date can be found on the Certificate of Analysis.

  2. How do I get lot-specific information or a Certificate of Analysis?

    The lot specific COA document can be found by entering the lot number above under the "Documents" section.

  3. How do I find price and availability?

    There are several ways to find pricing and availability for our products. Once you log onto our website, you will find the price and availability displayed on the product detail page. You can contact any of our Customer Sales and Service offices to receive a quote.  USA customers:  1-800-325-3010 or view local office numbers.

  4. What is the Department of Transportation shipping information for this product?

    Transportation information can be found in Section 14 of the product's (M)SDS.To access the shipping information for this material, use the link on the product detail page for the product. 

  5. Why is Product 157260, Hydroxybenzotriazole hydrate wet?

    Hydroxybenzotriazole hydrate is a solid that is explosive when dry. Our specification for this product is >14% water.

  6. Can Product 157260, Hydroxybenzotriazole hydrate, be dried?

    Drying hydroxybenzotriazole hydrate should not be attempted because of its explosive nature.

  7. How is Product 157260, Hydroxybenzotriazole hydrate, shipped?

    Hydroxybenzotriazole hydrate can not travel be sea or air. It is typically shipped by truck.

  8. My question is not addressed here, how can I contact Technical Service for assistance?

    Ask a Scientist here.

Tetrahedron Letters, 35, 3315-3315 (1994)
T Katoh et al.
International journal of peptide and protein research, 42(3), 264-269 (1993-09-01)
3-Dimethylphosphinothioyl-2(3H)-oxazolone (MPTO) was synthesized, and its ability to effect racemization-free couplings and cyclization of a peptide and its C-terminal epimer was examined. MPTO showed good reactivity in aprotic polar solvents such as N,N-dimethylformamide (DMF) and N-methylpyrrolidone. In reactivity MPTO resembles
Synlett, 733-733 (1993)
Tetrahedron Letters, 34, 6383-6383 (1993)
Akul Y Mehta et al.
Cell chemical biology, 27(9), 1207-1219 (2020-07-02)
Glycan recognition is typically studied using free glycans, but glycopeptide presentations represent more physiological conditions for glycoproteins. To facilitate studies of glycopeptide recognition, we developed Glyco-SPOT synthesis, which enables the parallel production of diverse glycopeptide libraries at microgram scales. The
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