SLB-5ms, 30 m x 0.25 mm I.D., 0.25 μm (28471-U)
40 °C (2 min), 22 °C/min to 240 °C, 10 °C/min to 330 °C (1 min)
250 °C
FID, 330 °C
helium, 30 cm/sec @ 200 °C, set using methane
0.5 μL splitless (0.75 min)
4 mm I.D., single taper
50 ng on-column of a 72 component semivolatile standard and 8 surrogate compounds, plus 6 internal standards (at 40 ng on-column), in methylene chloride
SLB is a registered trademark of Merck KGaA, Darmstadt, Germany