GC Analysis of Column Bleed on SLB^®-IL60 using FID, Comparison to 5 Polyethylene Glycol (PEG) Columns

column

30 m x 0.25 mm I.D., 0.25 μm

column

SLB-IL60, 30 m x 0.25 mm I.D., 0.20 μm (29505-U)

oven

50 °C (2 min), 15 °C/min to column programmed temperature limit (10

inj. temp.

250 °C

detector

FID, at column programmed temperature limit

carrier gas

helium, 1 mL/min

injection

1.0 μL splitless

liner

4 mm I.D., split/splitless type, single taper wool packed FocusLiner^™ design

sample

methylene chloride