GC Analysis of PCB Congeners in Stream Sediment on SPB^®-Octyl after SPME using 100 μm PDMS Fiber

sample/matrix

5 g stream sediment, downstream from industrial sites

SPME fiber

PDMS, 100 μm (57300-U) (57300-U)

extraction

headspace, 90 °C/30 min

desorption process

280 °C/2 min, splitless

column

SPB^®-Octyl, 30 m × 0.25 mm I.D., 0.25 μm (24218-U)

oven

50 °C/1 min at 10 °C/min to 150 °C/0 min