GC Analysis of QA Test Mix on SLB^®-IL60 before/after Carrier Gas Flow Stopped

column

SLB-IL60, 30 m x 0.25 mm I.D., 0.20 μm (29505-U)

oven

130 °C (25 min)

inj. temp.

250 °C

detector

FID, 250 °C

carrier gas

helium, 25 cm/sec

injection

1.0 μL 100:1 split

liner

4 mm I.D., split/splitless type, single taper wool packed FocusLiner^™ design

sample

polar column test mix (47302), 9 analytes, each at 500 μg/mL in methylene chloride