Equity-5, 30 m × 0.25 mm I.D., 0.5 μm (28092-U)
40 °C (2 min), 50 °C/min to 100 °C, 10 °C/min to 200 °C, 30 °C/min to 325 °C (7.5 min)
280 °C, splitless (0.61 min)
MSD, Scan range 45-450 amu, 325°C
helium, pressure programmed, 20 psi (0.0 min), ramp to 80 psi (0.0 min), ramp to 16.5 psi (3 min), ramp to 25 psi (hold for remainder of run)
1 μL, splitless (0.61 min)
4 mm I.D., single taper
50 ng on-column of a 62 Supplemental Appendix IX list consisting of semivolatile standards, 6 internal standards, and 8 surrogates
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