Astec CHIRALDEX B-TA, 30 m x 0.25 mm I.D., 0.12 μm (73023AST)
80 °C, 2 °C/min to 110 °C
250 °C
FID, 250 °C
helium, 30 psi
0.6 μL, 80:1 split
2.5 mg/mL each racemate in methanol (N-TFA derivatives)
Astec is a registered trademark of Merck KGaA, Darmstadt, Germany
CHIRALDEX is a trademark of Sigma-Aldrich Co. LLC