GC Analysis of Trichloroanisole (TCA) in Wine on SLB^®-5ms after SPME using 100 μm PDMS Fiber

材料

used together

产品编号

说明

价格

57928-U

SPME Fiber Assembly

100 μm PDMS, Metal Alloy (1 cm), needle size 23 ga, Autosampler, pk of 1, red hub

47526-U

2,4,6-Trichloroanisole solution

certified reference material, 100 μg/mL in methanol

28471-U

SLB^®-5ms Capillary GC Column

L × I.D. 30 m × 0.25 mm, d_f 0.25 μm

CONDITIONS

sample/matrix

red wine spiked with 5 ppt TCA

SPME fiber

100 μm PDMS metal fiber (57928-U)

extraction

headspace, room temp (30 min)

condition

3 min. at 250 °C

desorption process

250 °C for 3 min

column

SLB^®-5ms, 30 m x 0.25 mm I.D., 0.25 μm (28471-U)

oven

60 °C (2 min), 8 °C/min to 200 °C (10 min)

MSD interface

300 °C

scan range

SIM, m/z = 195, 197, 210, 212

carrier gas

helium, 1 mL/min. constant

liner

0.75 mm I.D. SPME

说明

法律信息

SLB is a registered trademark of Merck KGaA, Darmstadt, Germany

Chromatogram Search

Related Product Categories

HPLC Columns GC Columns & Accessories TLC Plates & Adsorbents Solid Phase Microextraction (SPME)Solid Phase Extraction & QuEChERS

Related Applications

Small Molecule HPLC Large Molecule HPLC Gas Chromatography (GC)TLC Solid Phase Microextraction (SPME)Solid Phase Extraction (SPE)QuEChERS

GC Analysis of Trichloroanisole (TCA) in Wine on SLB®-5ms after SPME using 100 μm PDMS Fiber

材料