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UHPLC Analysis of Flakka and Related Compounds on Titan Silica in HILIC Mode

UHPLC Analysis of Flakka and Related Compounds on Titan Silica in HILIC Mode suitable for HPLC

材料

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价格

3,4-亚甲基二氧吡咯烷酮盐酸盐(MDPV)标准液 CRM 溶液

1.0 mg/mL in methanol (as free base), ampule of 1 mL, certified reference material, Cerilliant®

MDPBP hydrochloride solution

1.0 mg/mL in methanol (as free base), ampule of 1 mL, certified reference material, Cerilliant®

Naphyrone hydrochloride

1.0 mg/mL in methanol (as free base), ampule of 1 mL, certified reference material, Cerilliant®

αα-盐酸吡咯烷基苯戊酮 盐酸盐 溶液

1.0 mg/mL in methanol (as free base), ampule of 1 mL, certified reference material, Cerilliant®

α-Pyrrolidinopropiophenone hydrochloride solution

1.0 mg/mL in methanol (as free base), ampule of 1 mL, certified reference material, Cerilliant®

CONDITIONS

column

Titan Silica, 10 cm x 2.1 mm I.D., 2 μm (581532-U)

mobile phase

10 mM ammonium formate in acetonitrile:water (95:5)

flow rate

0.4 mL/min

column temp.

35 °C

detector

UV, 265 nm

injection

1 μL

sample

50 μg/mL in methanol:acetonitrile (10:90)

说明

分析说明

The rapid separation of the street drug Flakka (α-PVP) and related compounds is shown here on a Titan Silica column in HILIC mode. Highest grade UHPLC solvents were used to supply low background interference and low particulate contamination for robust, trouble-free operation. Cerilliant CRMs provided reliable identification and quantification.

法律信息

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