SLB-5ms, 30 m x 0.25 mm I.D., 0.25 μm (28471-U)
40 °C (2 min), 22 °C/min to 240 °C, 10 °C/min to 330 °C, (1 min)
250 °C
330 °C
m/z = 40-450
helium, 1.0 mL/min (11 min), 10 mL/min to 1.5 mL/min (hold remainder of run)
0.5 μL, splitless (0.50 min)
2 mm I.D., straight
50 ng on-column of a 72 component semivolatile standard and 8 surrogate compounds, plus 6 internal standards (at 40 ng on-column)
SLB is a registered trademark of Merck KGaA, Darmstadt, Germany