SLB-5ms, 30 m x 0.25 mm I.D., 0.25 μm (28471-U)
40 °C (2 min), 15 °C/min to 240 °C, 10 °C/min to 330 °C (2 min)
250 °C
330 °C
m/z = 40-450
helium, 1.0 mL/min (11 min), ramp to 1.5 mL/min (constant for remainder of run)
1 μL, pulsed splitless (15 psi until 0.10 min), (0.75 min)
4 mm I.D., single taper
50 ppm of an 80 component semivolatile standard, plus 6 internal standards (at 40 ppm) in methylene chloride
SLB is a registered trademark of Merck KGaA, Darmstadt, Germany