LC/MS Analysis of Isobaric Bath Salts Mephedrone, Buphedrone, N-Ethylcathinone and MDAI on Ascentis® Express HILIC

材料
used together
产品编号
说明
价格
相关产品
产品编号
说明
价格
Buphedrone hydrochloride solution
1.0 mg/mL in methanol (as free base), ampule of 1 mL, certified reference material, Cerilliant®Mephedrone hydrochloride solution
1.0 mg/mL in methanol (as free base), ampule of 1 mL, certified reference material, Cerilliant®MDAI hydrochloride solution
100 μg/mL in acetonitrile: water (9:1) with 5% 1 M HCl (as free base), ampule of 1 mL, certified reference material, Cerilliant®N-Ethylcathinone hydrochloride solution
1.0 mg/mL in methanol (as free base), ampule of 1 mL, certified reference material, Cerilliant®CONDITIONS
column
Ascentis Express HILIC, 5 cm x 2.1 mm I.D., 2.7 μm particles (53934-U)
mobile phase
5 mM ammonium formate (98:2 acetonitrile:water)
flow rate
0.6 mL/min
pressure
1262 psi (87 bar)
column temp.
35 °C
detector
ESI(+), 178 m/z
injection
1 μL
sample
20 ng/mL
说明
法律信息
Ascentis is a registered trademark of Merck KGaA, Darmstadt, Germany