each analyte at 50 ppb in 5 mL water
PURGE TRAP K, O.I. ANALYTICAL 4560 (24940-U)
40 mL/min at 25 °C for 11 min
2 min
205 °C
210 °C for 2 min, 31 mL/min
260 °C for 10 min
110 °C
SPB-624, 30 m x 0.25 mm I.D., 1.4 μm (24255)
40 °C (2 min), 7 °C/min to 135 °C, 30 °C/min to 230 °C (3 min)
150 °C
200 °C
m/z = 35-350
helium, 1.2 mL/min
30:1 split
0.75 mm I.D. SPME
SPB is a registered trademark of Merck KGaA, Darmstadt, Germany