HPLC Analysis of Aminoglutethimide Enantiomers on Astec® Cellulose DMP
CONDITIONS
column
Astec Cellulose DMP; 25 cm x 4.6 mm I.D., 5 μm particles (51099AST)
mobile phase
[A] heptane; [B] isopropanol; [C] diethylamine; (70:30:0.1, A:B:C)
flow rate
1 mL/min
column temp.
30 °C
injection
15 μL
sample
aminoglutethimide, 1 g/L in 50:50, heptane:isopropanol
说明
分析说明
Aminoglutethimide enantiomers are resolved by normal phase chromatography.
法律信息
Astec is a registered trademark of Merck KGaA, Darmstadt, Germany