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LC/MS Analysis of Antifungals on Ascentis® Express Phenyl-Hexyl

LC/MS Analysis of Antifungals on Ascentis® Express Phenyl-Hexyl application for HPLC

材料

used together

产品编号
说明
价格

乙酸铵

LiChropur, eluent additive for LC-MS

相关产品

产品编号
说明
价格

Ascentis® Express Phenyl-Hexyl,2.7μm HPLC色谱柱

L × I.D. 10 cm × 2.1 mm, pk of 1 ea

氟康唑标准液 溶液

2.0 mg/mL in methanol, ampule of 1 mL, certified reference material, Cerilliant®

Itraconazole solution

2.0 mg/mL (Methanol with 1% 1M HCl), ampule of 1 mL, certified reference material, Cerilliant®

泊沙康唑标准液 溶液

2.0 mg/mL in methanol, ampule of 1 mL, certified reference material, Cerilliant®

伏立康唑标准液 溶液

2.0 mg/mL in methanol, ampule of 1 mL, certified reference material, Cerilliant®

酮康唑 溶液

2.0 mg/mL in methanol, ampule of 1 mL, certified reference material, Cerilliant®

CONDITIONS

column

Ascentis Express Phenyl-Hexyl, 10 cm x 2.1 mm I.D., 2.7 μm particles (53336-U)

gradient

[A] 10 mM ammonium acetate; [B] acetonitrile

gradient

2% B for 1 min; to 100% B in 10 min; held at 100% B for 1 min

flow rate

0.3 mL/min

pressure

2930 psi (202 bar)

column temp.

35 °C

detector

MS, ESI+, XIC

injection

0.5 μL

sample

Antifungals, 1-10 μg/mL in 99:1, water:methanol

说明

法律信息

Ascentis is a registered trademark of Merck KGaA, Darmstadt, Germany