LC/MS Analysis of Combination Drug Panel on Ascentis® Express Biphenyl

材料
used together
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说明
价格
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产品编号
说明
价格
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500 μg/mL in acetonitrile: water (1:1), ampule of 1 mL, certified reference material, Cerilliant®Zopiclone-N-oxide solution
100 μg/mL (Methanol with 1% 1 M HCl), ampule of 1 mL, certified reference material, Cerilliant®N-Desmethylzopiclone solution
100 μg/mL in acetonitrile, certified reference material, Cerilliant®CONDITIONS
column
Ascentis Express Biphenyl, 5 cm x 2.1 mm I.D., 2.7 μm particles (64057-U)
mobile phase
[A] 5 mM ammonium formate, 0.1% formic acid in water; [B] 5 mM ammonium formate, 0.1% formic acid in water:methanol (5:95)
gradient
5% B for 1 min; to 100% B in 5 min; held at 100% B for 1 min
flow rate
0.5 mL/min
pressure
431 psi (29.8 bar)
column temp.
25 °C
detector
MS, ESI+, EIC
injection
1 μL
sample
300 ng/mL in urine after dilution 9:1 in water
说明
法律信息
Ascentis is a registered trademark of Merck KGaA, Darmstadt, Germany