跳转至内容
Merck
CN

LC/MS Analysis of Combination Drug Panel on Ascentis® Express Biphenyl

LC/MS Analysis of Combination Drug Panel on Ascentis® Express Biphenyl application for LC-MS

材料

used together

产品编号
说明
价格

甲酸铵

eluent additive for LC-MS, LiChropur, ≥99.0%

相关产品

产品编号
说明
价格

芬太尼标准液 溶液

1.0 mg/mL in methanol, ampule of 1 mL, certified reference material, Cerilliant®

哌甲酯 盐酸盐 溶液

(Racemic mixture), ampule of 1 mL, 1.0 mg/mL in methanol (as free base), certified reference material, Cerilliant®

去甲羟吗啡酮 盐酸盐 溶液

1.0 mg/mL in methanol: DMSO (80:20) (as free base), ampule of 1 mL, certified reference material, Cerilliant®

去甲芬太尼标准液 草酸酯 溶液

1.0 mg/mL in methanol (as free base), ampule of 1 mL, certified reference material, Cerilliant®

羟考酮标准液 溶液

1.0 mg/mL in methanol, ampule of 1 mL, certified reference material, Cerilliant®

Oxymorphone-D3 solution

1.0 mg/mL in methanol, ampule of 1 mL, certified reference material, Cerilliant®

Pregabalin solution

1.0 mg/mL in methanol, ampule of 1 mL, certified reference material, Cerilliant®

利太林酸 盐酸盐 溶液

1.0 mg/mL in methanol (as free base), ampule of 1 mL, certified reference material, Cerilliant®

左匹克隆标准液 溶液

1.0 mg/mL in acetonitrile, ampule of 1 mL, certified reference material, Cerilliant®

扎来普隆标准液 溶液

1.0 mg/mL in methanol, ampule of 1 mL, certified reference material, Cerilliant®

唑吡坦苯基-4-羧酸 溶液

500 μg/mL in acetonitrile: water (1:1), ampule of 1 mL, certified reference material, Cerilliant®

Zopiclone-N-oxide solution

100 μg/mL (Methanol with 1% 1 M HCl), ampule of 1 mL, certified reference material, Cerilliant®

N-Desmethylzopiclone solution

100 μg/mL in acetonitrile, certified reference material, Cerilliant®

Ascentis® Express Biphenyl Column

2.7 μm particle size, L × I.D. 5 cm × 2.1 mm

CONDITIONS

column

Ascentis Express Biphenyl, 5 cm x 2.1 mm I.D., 2.7 μm particles (64057-U)

mobile phase

[A] 5 mM ammonium formate, 0.1% formic acid in water; [B] 5 mM ammonium formate, 0.1% formic acid in water:methanol (5:95)

gradient

5% B for 1 min; to 100% B in 5 min; held at 100% B for 1 min

flow rate

0.5 mL/min

pressure

431 psi (29.8 bar)

column temp.

25 °C

detector

MS, ESI+, EIC

injection

1 μL

sample

300 ng/mL in urine after dilution 9:1 in water

说明

法律信息

Ascentis is a registered trademark of Merck KGaA, Darmstadt, Germany