Titan C18, 10 cm x 2.1 mm I.D., 1.9 μm particles (577124-U)
(A) water; (B) acetonitrile, both with 0.1% formic acid
40%B for 1 min, to 90%B in 0.5 min, held for 2 min
0.4 mL/min
4500 psi (310 bar)
MS, ESI(+), MRM
2.0 μL
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